微波辐照法大规模合成梭状氧化铜纳米晶
Large scale synthesis of shuttle like CuO nanocrystals by microwave irradiation
氧化铜作为一种脱硫剂而具有重要研究意义。本文采用微波辐照法，醋酸铜为原料、氢氧化钠溶液为沉淀剂、直接使用水溶液为分散剂的制备出梭状氧化铜纳米晶。采用X射线衍射（XRD）、拉曼（Raman）光谱、X射线光电子能谱（XPS）、透射电子显微镜（TEM）和场发射扫描电子显微镜（FETEM）等对纳米氧化铜进行了表征，结果表明所得氧化铜产品具有单斜晶形梭状O/Cu比为1.026的氧化铜纳米晶。。
Nanocrystalline CuO with shuttle-morphology has been prepared conventionally by a microwave irradiation heating technique from an aqueous system in the presence of Cu(CH3COO)2o H2O and NaOH at room temperature. The X-ray powder diffraction pattern indicates that the product is indicated that the product was pure monoclinic phase of CuO. Further characterized by transmission electron microscopy, selected area electron diffraction, X-ray photoelectron spectroscopy and Raman spectra, the component of the products were confirmed.
张丽、王浩、蔡佩君、刘丽华
化学材料科学金属元素无机化合物化学工业
氧化铜微波辐照合成
upric oxideMicrowave irradiationSynthesis
张丽,王浩,蔡佩君,刘丽华.微波辐照法大规模合成梭状氧化铜纳米晶[EB/OL].(2010-07-07)[2025-08-11].http://www.paper.edu.cn/releasepaper/content/201007-141.点此复制
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