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石墨烯负载铁酸锌纳米材料的制备及应用

Preparation and application of ZnFe2O4/rGO

中文摘要英文摘要

本论文采用溶剂热方法一步合成了纳米复合材料ZnFe2O4/rGO,并将其修饰在玻碳电极表面,进行电化学性能测试。石墨烯的大比表面积与铁酸锌的多孔结构一定程度上促进了H2O2的还原。实验旨在最优化实验条件下研究催化剂电还原H2O2的行为。并采用SEM,TEM,XRD,XPS等手段对复合物进行了表征。石墨烯和ZnFe2O4之间的协同作用进一步提高了催化活性。该修饰电极制备方法简单、环保、快速,并具有良好的稳定性,将其应用到H2O2检测体系中,实现了H2O2的定量分析与检测。

In this paper, ZnFe2O4/rGO nanocompositewas synthesized by solvothermal method and modified on the surface of glassy carbon electrode. The electrochemical performance was tested. The large specific surface area of graphene and the porous structure of zinc ferrite promote the reduction of H2O2 to a certain extent. The aim of the experiment was to optimize the experimental conditions to study the electrocatalytic activity of H2O2. The composites were characterized by SEM, TEM, XRD and XPS. The synergistic effect between graphene and ZnFe2O4 further improves the catalytic activity. The preparation method of the modified electrode is simple, environmentally friendly, fast, and has good reproducibility and stability. It is applied to the H2O2 detection system to realize the quantitative detection of H2O2.

范晓彬、张国亮、宁凌云、李阳、彭文朝、张凤宝

化学

石墨烯铁酸锌过氧化氢

graphenezinc ferritehydrogen peroxide

范晓彬,张国亮,宁凌云,李阳,彭文朝,张凤宝.石墨烯负载铁酸锌纳米材料的制备及应用[EB/OL].(2017-04-28)[2025-08-02].http://www.paper.edu.cn/releasepaper/content/201704-798.点此复制

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