微波辅助水蒸汽加热法合成片层二硫化钼

In this paper, inexpensive sodium molybdate, thiourea and deionized water are used as raw materials and placed in the designed reactor. Using a domestic microwave oven, the solution is heated to volatilize the liquid water into water vapor. Under the action of microwave, the water vapor generates a temperature much higher than that of the liquid water, so that the sheet of molybdenum disulfide is rapidly synthesized in 5 minutes. The morphological structures were characterized by XRD, Raman spectra, SEM, TEM, AMF and nitrogen adsorption-desorption experiments. Due to the steam heating, the synthesized molybdenum disulfide does not agglomerate due to the presence of liquid water, and only forms a two-dimensional structure in which the sheets are stacked.