激光区熔定向凝固Al2O3/Y3Al5O12(YAG)
irectionally solidified Al2O3/Y3Al5O12 (YAG) eutectic ceramic in-situ composite by laser remelting
采用高能激光束作为定向凝固的热源,从熔体中直接制备Al2O3/Y3Al5O12(YAG)共晶自生复合陶瓷,研究了其在超高温度梯度下的凝固组织特征以及与激光工艺参数的关系,并对其力学性质进行了分析。研究结果表明:(1)凝固组织强烈的受激光扫描速率与功率密度的影响。当二者匹配时,Al2O3相和Y3Al5O12(YAG)相呈现均匀一致,各向同性,连续分布的层状耦合共晶结构,共晶间距细小(1-2um),且随扫描速率的增大逐渐减小。(2) 实验制备的Al2O3/Y3Al5O12(YAG)共晶陶瓷硬度高达19.84 Gpa,断裂韧性达到3.72 KIC/MPa.m1/2。
With the high-energy laser as heat resource for directional solidification, Al2O3/(Y3Al5O12)YAG eutectic ceramic was rapidly prepared from melt in this paper. The relationship between the eutectic microstructure and the processing parameters is studied, and the mechanical property of the composite is preliminarily investigated. The results show that: (1) The scanning rate and power density strongly affect the eutectic microstructure. With the processing parameters adjusted properly, the binary Al2O3/YAG has an uniform and homogeneous lamella microstructure , in which single crystal Al2O3,single-crystal YAG are three-dimensionally and continuously reticular connected and finely coupled without grain boundaries ,colonies and amorphous phases between interfaces. Eutectic spacing reduces with scanning rate’s increasing and is only around 1-2 um. (2) The maximum hardness reaches 19.84Gpa and the room fracture toughness were attained for 3.72 MPa.m1/2 by vickers indentation method.
刘林、苏海军、张军
材料科学晶体学
l2O3/Y3Al5O12(YAG)共晶自生复合陶瓷激光区熔
l2O3/Y3Al5O12 (YAG)eutectic ceramic in-situ compositelaser remelting
刘林,苏海军,张军.激光区熔定向凝固Al2O3/Y3Al5O12(YAG)[EB/OL].(2005-08-04)[2025-08-18].http://www.paper.edu.cn/releasepaper/content/200508-36.点此复制
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