中药复方四逆散水煎物HPLC指纹图谱研究
Studies on HPLC Fingerprint Chromatogram of Decoction of sinisan
用HPLC方法，使用kromasil－C18色谱柱（4.6mm╳250mm，5μm），以乙腈－0.05％磷酸水梯度洗脱，检测波长为240nm、210nm，流速为1.0ml/min构建了复方四逆散水煎物HPLC指纹图谱，对指纹图中四个主要成分峰进行了初步定性，为其质量控制提供参考，并为其化学成分研究奠定基础。
HPLC finger-print chromatograph of decoction of sinisan was set up by the method of HPLC and by means of Kromasil C18 Column（4.6mm╳250mm，5μm）.The condition of HPLC: Acetonitrile-0.05％ Phosphoric acid water solvent gradient programming, wavelength, 240nm、210nm of and flow rate,1.0 ml·min-1. Four main compositions were confirmed initially. The HPLC finger-print chromatograph can be used to control the quality of decoction of sinisan and eatablish the foundation for the chemical compositons researching.
李廷利、黄玉新、都晓伟
药学中医学医学研究方法
四逆散指纹图谱HPLC
decoction of sinisanHPLCfingerprint chromatograph
李廷利,黄玉新,都晓伟.中药复方四逆散水煎物HPLC指纹图谱研究[EB/OL].(2006-03-03)[2025-07-19].http://www.paper.edu.cn/releasepaper/content/200603-43.点此复制
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