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多孔金刚石坯体熔渗铜工艺研究

Study on process of copper infiltration into porous diamond preforms

中文摘要英文摘要

金刚石/Cu具有优异的热物理性能,采用熔渗法可以实现金刚石/Cu的近净成形。多孔金刚石坯体熔渗铜的相关工艺及影响因素在本文中做了主要研究。研究结果表明,在多孔坯体上下方都放置铜块时对于熔渗过程比较有利,熔渗温度达到1200℃时,压力20MPa,保温30分钟复合材料致密度达到99.8%,接近全致密,导热率可以达到587 W/moK,进一步提高熔渗温度和延长保温时间复合材料的致密度没有显著变化,但导热率将下降,这主要与界面结构的变化而引起界面热阻变化有关。熔渗过程存在孕育期,熔渗温度低于1200℃或压力低于20MPa时,复合材料的致密度较低,甚至不能完成熔渗。

iamond / copper composites have good thermal-physical properties and they could be net-shape formed by infiltration. In this research, relevant process and influencing factors of porous diamond preforms infiltrated by copper were studies. The results showed that it is helpful to infiltration of copper into diamond preforms when the copper were both placed on the top and at the bottom of the preform. The density of the composites could reach 99.8% near full density at 1200 C with the pressure of 20MPa for 30 min and thermal conductivity can reach 587 W / m o K. There is no obvious change for the density by further incerasing the infiltration temperature and holding time. But the thermal conductivity droped. This was associated with the increase of interfacial thermal resistance due to the change of interface structure. There is an incubation period during the pressure infiltration process. The density was lower when infiltration temperature was below 1200 C or pressure was less than 20MPa, even that infiltration can not be completed.

曲选辉、李改、郭彩玉、何新波、许慧、任淑彬

材料科学

金属基复合材料多孔金刚石坯体熔渗导热率

Metal matrix compositesporous diamond preformsinfiltrationthermal conductivity

曲选辉,李改,郭彩玉,何新波,许慧,任淑彬.多孔金刚石坯体熔渗铜工艺研究[EB/OL].(2012-05-02)[2025-08-29].http://www.paper.edu.cn/releasepaper/content/201205-10.点此复制

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