空气氧化法制备正八面体纳米Fe3O4
Preparation of octahedral magnetic nanoparticles by air oxidation
本论文利用空气部分氧化Fe2+,在碱性条件下,简单快速的制备出具有正八面体形貌的磁性纳米Fe3O4粒子,其性能非常稳定,可长期暴露于空气中不被氧化。用傅立叶红外光谱(FT-IR)、X射线衍射(XRD)、扫描电镜(SEM)、量子扰动超导探测(SQUID)等手段对该纳米材料进行了表征。结果表明,Fe3O4呈规则的正八面体形貌,正八面体棱长在35nm左右,室温下具有超顺磁性,饱和磁化强度Ms为75emμ/g。
In this paper, octahedral magnetic nanoparticles have been prepared by precipitation from partially oxidated Fe2+ using air as natural oxidant, which are superparamagnetic and have high stablity in the air. The product was characterized by means of Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscopy, and. superconductivity quantum Interference device. The results show that, the morphology is octahedron, and the average edge length of Fe3O4 is about 30nm, in addition, it is superparamagnetic in the room temperature and the saturation magnetization is 75emμ/g .
谢安建、王娟、沈玉华
材料科学化学电化学工业
空气氧化正八面体纳米Fe3O4
air oxidationoctahedralnanomagnetic
谢安建,王娟,沈玉华.空气氧化法制备正八面体纳米Fe3O4[EB/OL].(2010-04-28)[2025-08-17].http://www.paper.edu.cn/releasepaper/content/201004-1057.点此复制
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