一种简单的方法制备介孔二氧化钛/石墨碳纳米微球
simple nanocasting route for preparation of mesoporous titanium dioxide/GCM microsphere
以二氧化硅微球作为模板，通过一种简单的纳米铸型方法，制备了二氧化钛/石墨碳纳米微球。采用X射线衍射仪(XRD)、比表面积分析仪（BET）、场发射扫描电子显微镜(SEM) 、透射电子显微镜（TEM）、差热分析仪（TG-DAT）等仪器和检测方法，对二氧化钛/石墨碳纳米微球的形貌和结构进行表征。实验分析结果表明：得到的碳材料石墨化程度较好，锐钛矿型二氧化钛纳米颗粒较好地分散于石墨碳微球载体中，且钛矿型二氧化钛颗粒直径约为8-14 nm。所制备的材料可以用作光催化剂和电池材料。
Mesoporous titanium dioxide/graphitic carbon microspheres were synthesized by a simple nanocasting route using monodisperse silicon dioxide microspheres as the template. The characterize and the morphology of the titanium dioxide/graphitic carbon microspheres have been analyzed by means of XRD, N2-sorption, SEM, TEM, TG-DTA and EDAX. Indicated by the experimental results and the theoretical analysis, the anatase titanium dioxide nanoparticles of 8-14 nm in diameter were highly dispersed in the graphitic carbon microspheres. The obtained material can be used as catalyst or battery material.
李溪、张成丽、康诗飞
材料科学无机化学工业非金属元素化学工业、非金属无机化合物化学工业
二氧化钛/石墨碳纳米微球纳米铸型介孔
titanium dioxide/graphitic carbonMicrospheresNanocasting routeMesoporous
李溪,张成丽,康诗飞.一种简单的方法制备介孔二氧化钛/石墨碳纳米微球[EB/OL].(2012-12-24)[2025-08-23].http://www.paper.edu.cn/releasepaper/content/201212-688.点此复制
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