NiFe2Ox@C微波辅助燃烧合成及其吸附脱硫性能研究

NiFe2Ox@C composites have been obtained by means of a microwave-assisted combustion synthesis mediated. The structure of the materials were characterized by X-ray diffraction, transmission electron microscopy and alternating gradient magnetometer. The results show that the size of the metal oxide is about 20 nanometers with mainly spinel structure and solid bulk phase distribution characters in carbon. At room temperature, magnetic hysteresis loops at an applied field of 10 kOe show small coercivities, indicating the ferromagnetic behavior of the as-prepared NiFe2Ox@C composite with saturation magnetization of 59.6 emu/g. The resulting materials were found to be a promising candidate for adsorption desulfurization of dibenzothiophene (DBT) with a maximum adsorption capacity of 26.9 mgS/g from DBT-n-octane mixture.